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| Cis Mesylate | CAS 67914-86-7 | |
|---|---|---|
| Test | Specification |  |
| Description | A white to off-white colour crystalline. | |
| Identification by A) HPLC | The retention time of the major peak in the chromatogram of test solution should correspond to that of the standard solution | |
| B) IR | The Infra-red absorption spectrum of the sample should exhibit maxima only at the same wavelengths as that of a similar preparation of working standard | |
| Solubility | Freely soluble in Dichloromethane, Dimethyl formamide and in chloroform Soluble in Methanol | |
| Moisture Content | Not more than 0.5 %w/w | |
| Melting Range | Between 91 to 99ºC | |
| Related substances by HPLC | ||
| IT-IT8 | Not more than 0.30% | |
| Cis Bromo Benzoate | Not more than 0.30% | |
| Trans Bromo Benzoate | Not more than 0.30% | |
| Impurity about RRT 0.77 | Not more than 0.30% | |
| Any other unknown Impurity | Not more than 0.50% | |
| Total Impurity | Not more than 1.00% | |
| Assay (on anhydrous basis) | Not less than 98.0% | |
| Cis Mesylate | |
|---|---|
| CAS 67914-86-7 | |
| |
|
| Test | Specification |
| Description | A white to off-white colour Crystalline. |
| Identification by A) HPLC | The retention time of the major peak in the chromatogram of test solution should correspond to that of the standard solution |
| B) IR | The Infra-red absorption spectrum of the sample should exhibit maxima only at the same wavelengths as that of a similar preparation of working standard |
| Solubility | Freely soluble in Dichloromethane, Dimethyl formamide and in chloroform Soluble in Methanol |
| Moisture Content | Not more than 0.5 %w/w |
| Melting Range | Between 91 to 99ºC |
| Related substances by HPLC | |
| IT-IT8 | Not more than 0.30% |
| Cis Bromo Benzoate | Not more than 0.30% |
| Trans Bromo Benzoate | Not more than 0.30% |
| Impurity about RRT 0.77 | Not more than 0.30% |
| Any other unknown Impurity | Not more than 0.50% |
| Total Impurity | Not more than 1.00% |
| Assay (on anhydrous basis) | Not less than 98.0% |
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